HCID 2292631, compound → HCID 22760589, compound

HRID 1703876Notes

Reaction equation

HRID 1703876 reaction equation
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH2:16]([NH:19][C:20]([NH:22][CH2:23][C:24]1[CH:25]=[N:26][CH:27]=[CH:28][CH:29]=1)=[S:21])[CH:17]=[CH2:18]>>[BrH:1].[CH2:16]([N:19]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)([OH:4])[CH2:2][S:21][C:20]1=[N:22][CH2:23][C:24]1[CH:25]=[N:26][CH:27]=[CH:28][CH:29]=1)[CH:17]=[CH2:18]

Participants

3

Reactant 2

HCID 2292631HCID 2292631, compoundHCID 12952390Bromo-4'-chloro-3'-sulfamoylacetophenone

Product 1

HCID 22760589HCID 22760589, compound

Procedure

4.7 g of 2-bromo-4'-chloro-3'-sulfamoylacetophenone and 3 g of 1-allyl-3-(3-pyridylmethyl)-thiourea were reacted as prescribed in Example 23 and the end product was filtered off. Colorless solid body, decomposition beginning at 82° C. γC=N 1605 cm-1.

Workup

  1. filtrationthe end product was filtered off
  2. customat 82° C.

Sources & evidence

ORD record
ord-b60aca94b4eb437aaade58288b9f5bef
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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