HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diazomethane → 4'-Methyl-3'-sulfamoyl-diazoacetophenone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diazomethane | HCID 9550 | — |
| Edukt | 4-Methyl-3-sulfamoyl-benzoyl chloride | HCID 22760560 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 4'-Methyl-3'-sulfamoyl-diazoacetophenone | HCID 54047535 | — |
Reaktionsschritte
12 g of 4-methyl-3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66(b) with diazomethane in diethyl ether and the substance precipitating as fair yellow precipitate was filtered off. Melting point: 176° C. (decomposition).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04125614 |
| Quelldatensatz | uspto-grants-1978_11 |
| ORD ID | ord-38cf729c823e4c5ab1cf67812875718c |
| Quellennotiz | uspto-grants-1978_11 |