HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Diethylthiourea → 3-Ethyl-2-ethylimino-4-(4-isopropyl-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Diethylthiourea | HCID 2735009 | — |
| Reactant | 2-Chloro-4'-isopropyl-3'-sulfamoylacetophenone | HCID 22760666 | — |
| Product | 3-Ethyl-2-ethylimino-4-(4-isopropyl-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride | HCID 22760671 | — |
Reaction Steps
5.5 g of 2-chloro-4'-isopropyl-3'-sulfamoylacetophenone and 2.2 g of 1,3-diethylthio urea were reacted and worked up as prescribed in Example 12. Colorless solid body, decomposition beginning at 96° C., γ C=N 1610 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125614 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-9fcc37e39b724ef8b1664c139446fcdb |
| Source note | uspto-grants-1978_11 |