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HRID1703892

反应详情

EQUATION

反应方程式

HRID 1703892 的结构方程式

REACTANTS

反应物

2
结构：C=[N+]=[N-]
HCID9550

Diazomethane

CH2N2

结构：NS(=O)(=O)c1cccc(C(=O)Cl)c1
HCID18801883

未命名化合物

PRODUCTS

生成物

1
结构：[N-]=[N+]=CC(=O)c1cccc(S(N)(=O)=O)c1
HCID53705814

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

11 g of 3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66(b) with diazomethane in diethyl ether and the crystals were filtered off. Melting point: 142° C.

WORKUP

后处理

  1. filtrationthe crystals were filtered off