N,N'-Dimethylthiourea → HCID 22760454, compound

HRID 1703912Notes

Reaction equation

HRID 1703912 reaction equation
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:21])(=[O:20])[NH:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH:6]=1)=[O:4].[CH3:22][NH:23][C:24]([NH:26][CH3:27])=[S:25]>>[BrH:1].[Cl:11][C:8]1[CH:9]=[CH:10][C:5]([C:3]2([OH:4])[CH2:2][S:25][C:24](=[N:23][CH3:22])[N:26]2[CH3:27])=[CH:6][C:7]=1[S:12](=[O:21])(=[O:20])[NH:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

3

Reactant 2

HCID 2723631N,N'-DimethylthioureaHCID 22760535HCID 22760535, compound

Product 1

HCID 22760454HCID 22760454, compound

Procedure

5.2 g of 2-bromo-4'-chloro-3'-phenylsulfamoylacetophenone and 1.5 g of 1,3-dimethylthiourea were reacted as prescribed in Example 23 and the precipitated end product was filtered off. Colorless crystals, melting point: 82° C. (decomposition).

Workup

  1. filtrationthe precipitated end product was filtered off

Sources & evidence

ORD record
ord-ca47214cce3b46b38982701bd774b81a
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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