N,N'-Dimethylthiourea → HCID 22760694, compound

HRID 1703931Notes

Reaction equation

HRID 1703931 reaction equation
[CH2:1]([N:3]([CH2:18][CH3:19])[S:4]([C:7]1[CH:8]=[C:9]([C:14](=[O:17])[CH2:15]Cl)[CH:10]=[CH:11][C:12]=1[Cl:13])(=[O:6])=[O:5])[CH3:2].[CH3:20][NH:21][C:22]([NH:24][CH3:25])=[S:23]>>[ClH:13].[Cl:13][C:12]1[CH:11]=[CH:10][C:9]([C:14]2([OH:17])[CH2:15][S:23][C:22](=[N:21][CH3:20])[N:24]2[CH3:25])=[CH:8][C:7]=1[S:4](=[O:6])(=[O:5])[N:3]([CH2:18][CH3:19])[CH2:1][CH3:2]

Participants

3

Reactant 2

HCID 2723631N,N'-DimethylthioureaHCID 22760643HCID 22760643, compound

Product 1

HCID 22760694HCID 22760694, compound

Procedure

4.8g of 3'-diethylsulfamoyl-2,4'-dichloroacetophenone and 1.5 g of 1,3-dimethylthiourea were reacted as prescribed in Example 23 and the crystalline end product was filtered off. Melting point: 165° C. (decomposition).

Workup

  1. filtrationthe crystalline end product was filtered off

Sources & evidence

ORD record
ord-1664ed66cd564570b1654b72cd502657
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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