N,N'-Dimethylthiourea → HCID 22760503, compound

HRID 1703932Notes

Reaction equation

HRID 1703932 reaction equation
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:21])(=[O:20])[N:13]([CH2:17][CH2:18][CH3:19])[CH2:14][CH2:15][CH3:16])[CH:6]=1)=[O:4].[CH3:22][NH:23][C:24]([NH:26][CH3:27])=[S:25]>>[ClH:1].[Cl:11][C:8]1[CH:9]=[CH:10][C:5]([C:3]2([OH:4])[CH2:2][S:25][C:24](=[N:23][CH3:22])[N:26]2[CH3:27])=[CH:6][C:7]=1[S:12](=[O:21])(=[O:20])[N:13]([CH2:17][CH2:18][CH3:19])[CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 2723631N,N'-DimethylthioureaHCID 22760461HCID 22760461, compound

Product 1

HCID 22760503HCID 22760503, compound

Procedure

4.8 g of 2,4'-dichloro-3'-dipropylsulfamoylacetophenone and 1.5 g of 1,3-dimethylthiourea were reacted as prescribed in Example 23 and worked up. Colorless crystals, melting point: 166° C. (decomposition).

Sources & evidence

ORD record
ord-ebe51a6790d54a0298233751f29ff631
Source dataset
uspto-grants-1978_11
Patent number
US04125614

Reaction notes

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