Bromine → HCID 22756413, compound

HRID 1703940Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:10])[CH3:9])=[CH:4][C:3]=1[S:11](=[O:17])(=[O:16])[NH:12][CH2:13][CH2:14][CH3:15].[Br:18]Br>>[Br:18][CH2:9][C:8]([C:5]1[CH:6]=[CH:7][C:2]([Cl:1])=[C:3]([S:11](=[O:17])(=[O:16])[NH:12][CH2:13][CH2:14][CH3:15])[CH:4]=1)=[O:10]

Participants

Reactant 2

HCID 24408Bromine

HCID 22760432HCID 22760432, compound

Product 1

HCID 22756413HCID 22756413, compound

Procedure

13.8 g of 4'-chloro-3'-propylsulfamoylacetophenone were reacted as described in Example 1(a) with 8 g of bromine to give the 2-bromo-4'-chloro-3'-propylsulfamoylacetophenone, melting point: 96° C., from isopropanol).

Sources & evidence

ORD record: ord-5287cdb0310e46c38eedcd5f227e5960
Source dataset: uspto-grants-1978_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04125614

Reaction notes

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