HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 328733, compound → HCID 23455710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 328733 | HCID 328733 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 23455710 | HCID 23455710 | — |
Reaction Steps
2-(3,4-Methylenedioxyphenyl)ethyl cyclopropyl carbinol [IV; Ar is 3,4-methylenedioxyphenyl, R is H] was prepared from 18.4 g. of 2-(3,4-methylenedioxyphenyl)vinyl cyclopropyl ketone (Preparation A2) and 3.1 g. of lithium aluminum hydride according to the procedure described above in Preparation B1, affording 11.5 g., b.p. 116°-122° C. (0.005 mm.), m.p. 64°-65° C. when recrystallized from ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125541 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-f87816dd07314413bfa85c7c04efb4b3 |
| Source note | uspto-grants-1978_11 |