HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 20392609, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Methyl [p-(phenoxy)phenyl]acetate | HCID 12531834 | — |
| Catalyst | Carbon Tetrachloride | HCID 5943 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 20392609 | HCID 20392609 | — |
Reaction Steps
A mixture of 22.68 g of methyl [p-(phenoxy)phenyl]acetate, 17.195 g of N-bromosuccinimide and 20 drops of carbon tetrachloride saturated with HBr in 300 ml of carbon tetrachloride is heated at reflux for 28 hours. After cooling, the mixture is filtered through aluminum oxide, concentrated and distilled at 0.15 mm to give the product as a colorless oil (bp 162.5°-165° C).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125729 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-7077b745b0ae4f0292ff282b5161c6c2 |
| Source note | uspto-grants-1978_11 |