HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 20392617, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Methyl α-bromo-4-iodobenzeneacetate | HCID 20392584 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20392617 | HCID 20392617 | — |
Reaction Steps
In a similar manner as in Example 29, 14.2 g of methyl α-bromo-α-(p-iodophenyl)acetate is reacted with 4.70 g of phenol in methanol to yield a white to light pink solid, mp 68°-71° C. Recrystallization from petroleum ether yields the product as white crystals, mp 72.5°-74° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125729 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-3d54bd1a23b14ed78343f46c5755e046 |
| Source note | uspto-grants-1978_11 |