HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenol → HCID 12531897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | HCID 20392605 | HCID 20392605 | — |
| Product | HCID 12531897 | HCID 12531897 | 62% |
Reaction Steps
In a manner similar to Example 16, 7.43 g of methyl α-bromo-α-[p-(p-chlorophenylthio)phenyl]acetate was reacted with 3.21 g of p-chlorophenol. Ether workup, chromatography and recrystallization from 150 ml of hexane:chloroform (15:1) yielded 5.2 g of a white solid, mp 90.5°-94.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125729 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-aef1122a856a4b4696a419d5f7c00f3a |
| Source note | uspto-grants-1978_11 |