HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(1-Methylcyclohexyl)phenol → HCID 90673584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(1-Methylcyclohexyl)phenol | HCID 13010975 | — |
| Reactant | Methyl alpha-Bromo-alpha-[p-(p-chlorophenoxy)phenyl]acetate | HCID 20392594 | — |
| Product | HCID 90673584 | HCID 90673584 | 79.6% |
Reaction Steps
In a manner similar to Example 16, 7.11 g of methyl α-bromo-α-[p-(p-chlorophenoxy)phenyl]acetate is reacted with 4.75 g of p-(1-methylcyclohexyl)phenol for 4 hrs. Chilling and filtering gives 7.4 g of product, mp 110°-112° C. Recrystallization from methanol-chloroform gives 6.3 g of white crystals, mp 111°-112.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125729 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-5c1745636b8c4eeb9305fcdf7441ce90 |
| Source note | uspto-grants-1978_11 |