HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → HCID 14171590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzeneacetic acid, 4-hydroxy-, methyl ester | HCID 518900 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 14171590 | HCID 14171590 | — |
Reaction Steps
A mixture of 47.4 g of methyl p-hydroxyphenylacetate, 28.5 ml of 3-bromo-1-chloropropane, 38.6 g of potassium carbonate and 700 ml of acetone is stirred and refluxed for 24 hours. The mixture is chilled, filtered and the solvent removed under reduced pressure. Distillation of the residue gives 52.1 g of colorless oil, bp 144°-146° C. at 0.25mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04125732 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-0ed8bc6735b84a7cad23dfe087e95b75 |
| Source note | uspto-grants-1978_11 |