Potassium Iodide → HCID 131711332, compound

Participants

Reaction Steps

As described in Example 30, a mixture of 5.2 g of m-phenoxyphenol, 1.06 g of 60% sodium hydride-oil dispersion, 3.82 g of potassium iodide, one ml of hexamethylphosphoramide and 10.4 g of methyl bromo{p-[3-(p-chlorophenoxy)propoxy]phenyl}acetate in 80 ml of tetrahydrofuran is refluxed for 18 hours and worked-up to give 13.6 g of gum. The gum is chromatographed over silica gel with dichloromethane as eluent to give 11.2 g of product as a viscous oil.

Provenance & Evidence