HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Ethyl-2-methylhexanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Ethyl-2-methylhexanoic acid | HCID 36646 | — |
| Product | 2-Ethyl-2-methylhexanoyl chloride | HCID 22759085 | 90.6% |
Reaction Steps
316 gm (2moles) of 2-methyl-2-ethyl-hexanoic acid were heated to boiling with 357 gm (3 moles) of thionyl chloride under agitation until the evolution of gas had ended. The surplus thionyl chloride was distilled off and the residue was fractionated in vacuo. 320 gm (90% of theory) of 2-methyl-2-ethyl-hexanoyl chloride of b.p. 78° C. at 13 mmHg were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04126585 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-bb0b75b6e1504d96ad029c34e941c93d |
| Source note | uspto-grants-1978_11 |