HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl mercaptan → HCID 54092293, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl mercaptan | HCID 7509 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 54070391 | HCID 54070391 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54092293 | HCID 54092293 | 63.3% |
Reaction Steps
Operating as described in Example 10, from 3 g of 1,7-dichloro-1-fluoro-hept-1-ene, 2.14 g of benzylmercaptan, 0.7 g of NaH (at 55% concentration in paraffin oil) and 30 ml of N,N-dimethylformamide there were obtained 2.8 g of product which was purified in a chromatography column.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04126623 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-ad19e95ffd084be9bb6233e20b6c1ef9 |
| Source note | uspto-grants-1978_11 |