HCID 22759221, compound → HCID 22759309, compound

HRID 1704355Notes

Reaction equation

HRID 1704355 reaction equation
O1CCCCC1[O:7][CH2:8]/[CH:9]=[CH:10]/[CH:11]([O:21][C:22](=[O:24])[CH3:23])[CH2:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([F:20])=[CH:16][CH:15]=1.C(C(CCCC(O)COC1C=CC(F)=CC=1)CC#CCCCC(O)=O)(=O)C>>[C:22]([O:21][CH:11]([CH2:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([F:20])=[CH:16][CH:15]=1)/[CH:10]=[CH:9]/[CH2:8][OH:7])(=[O:24])[CH3:23]

Participants

3

Reactant 2

HCID 22759221HCID 22759221, compoundHCID 22759232HCID 22759232, compound

Product 1

HCID 22759309HCID 22759309, compound

Procedure

The synthesis of this compound is carried out by the procedure of Example 4, Step B-5 except that an equivalent quantity of 1-(2-tetrahydropyranyloxy)-4-acetoxy-5-(4-fluorophenoxy)-trans-2-pentene is substituted for the 1-(2-tetrahydropyranyloxy)-4-acetoxy-5-(4-fluorophenoxy)pentane of Example 4, Step B-5. The product is obtained as a viscous oil.

Workup

  1. customThe synthesis of this compound
  2. customThe product is obtained as a viscous oil

Sources & evidence

ORD record
ord-79e8f73d7ccd4767905deb9af0799f90
Source dataset
uspto-grants-1978_11
Patent number
US04126629

Reaction notes

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