HCID 22759223, compound → HCID 22759279, compound

HRID 1704367Notes

Reaction equation

HRID 1704367 reaction equation
[C:1]([CH:4]([CH2:16][CH2:17][CH2:18][CH:19]([OH:28])[CH2:20][O:21][CH2:22][C:23]1[O:27][CH:26]=[CH:25][CH:24]=1)[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][C:11]([O:13]CC)=[O:12])(=[O:3])[CH3:2].C(C(CCCC(O)COC1C=CC(F)=CC=1)CCCCCCC(O)=O)(=O)C>>[C:1]([CH:4]([CH2:16][CH2:17][CH2:18][CH:19]([OH:28])[CH2:20][O:21][CH2:22][C:23]1[O:27][CH:26]=[CH:25][CH:24]=1)[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][C:11]([OH:13])=[O:12])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 22759223HCID 22759223, compoundHCID 22759241HCID 22759241, compound

Product 1

HCID 22759279HCID 22759279, compound

Procedure

The synthesis of this compound is carried out by the procedure of Example 1, Step F, except that an equivalent quantity of ethyl 8-acetyl-12-hydroxy-13-furfuryloxytridecanoate is substituted for the ethyl 8-acetyl-12-hydroxy-13-(4-fluorophenoxy)-tridecanoate of Example 1, Step F. The title compound is purified by chromatography on silica gel and is obtained as a yellow viscous oil.

Workup

  1. customThe synthesis of this compound
  2. customThe title compound is purified by chromatography on silica gel
  3. customis obtained as a yellow viscous oil

Sources & evidence

ORD record
ord-d594457c19254909aa141599cb136329
Source dataset
uspto-grants-1978_11
Patent number
US04126629

Reaction notes

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