HRID1704685

反应详情

EQUATION

反应方程式

HRID 1704685 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 20.0 g of 2-(3-dimethylaminopropoxy)-benzaldehyde and 10.3 g of benzylamine in 100 ml of toluene is heated at reflux for one hour in a procedure for Example 1. The yield of product is 22.1 g, boiling point 175°-178° C./0.05 mm of Hg.

WORKUP

后处理

  1. temperatureat reflux for one hour in a procedure for Example 1