N-(3-acetamido-5-aminophenyl)acetamide → HCID 178474334, compound

Participants

Reaction Steps

To a refluxing mixture of 0.96 g. (0.0045 mol) of 3,5-diacetyl-4,6-dihydroxy-2H-pyran-2-one in 35 ml. of methanol was added a solution of 1 g. (0.0045 mol) of 3,5-bis-acetamidoaniline (prepared as above) in 15 ml. of methanol. After three hours at reflux, the reaction mixture was cooled and filtered to yield 5-acetyl-4-hydroxy-3-[1-(3,5-bis-acetamidophenylamino)ethylidene]-2H-pyran-2,6(3H)-dione, m.p. 265°-267° C. (dec.).

Provenance & Evidence