HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenacyl bromide → HCID 70616701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenacyl bromide | HCID 7454 | — |
| Reactant | 5-ethyl-1,3,5-triazinane-2-thione | HCID 736590 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 70616701 | HCID 70616701 | — |
Reaction Steps
A solution of 6.95 grams (0.025 moles) of p-bromophenacylbromide in 60 milliliters of acetone was mixed with a solution of 3.62 grams (0.025 moles) of 5-ethyl 3,4,5,6-tetrahydro-s-triazin 2(1H) thione in 500 milliliters of acetone. After 10 minutes 6-p-bromophenyl-3-ethyl-6-hydroxy-3,4,6,7-tetrahydro-2H-thiazolo(3,2-a)-s-triazine hydrobromide crystallized out as a colourless solid, m.p. 132°-134° C. The yield was 9.27 grams (88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04127660 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-31930bd88d6e4b84b237130749783f00 |
| Source note | uspto-grants-1978_11 |