HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21333332, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 21333313 | HCID 21333313 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21333332 | HCID 21333332 | — |
Reaction Steps
Heat at reflux 4 gm. (0.01 mole) of cyanomethyl-5-(triphenylmethyl)picolinate and 2 ml. triethylamine in 50 ml. methanol for 4 hr. Remove methanol under reduced pressure. Triturate solid residue with water and recrystallize from ethylacetate - isopropyl ether, to obtain the product of this example, m.p. 160°-164°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04127662 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-1f1f9e1ea3f74b9b855340afd1632cf5 |
| Source note | uspto-grants-1978_11 |