N,N-Diethylethylenediamine → N(2-diethylaminoethyl)-5-butanoyl-2-methoxybenzamide

Participants

Reaction Conditions

Reaction Steps

In a flask equipped with a Dean-Stark device, there are introduced 10 g of the ester obtained in Example 3 and 10 g of diethylaminoethylamine and the mixture is heated to 100° C. for 3 hours. There are thus obtained 10.3 g of an oily product which is converted to hydrochlorate in the ethanol-ether mixture. The product obtained has a melting point of 155° C.

Provenance & Evidence