HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl Isothiocyanate → N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl Isothiocyanate | HCID 7673 | — |
| Reactant | 4-chloro-N-cyclopentylbenzylamine | HCID 834083 | — |
| Product | N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea | HCID 13018271 | 92.8% |
Reaction Steps
Analogously to Example 1, 21 grams (0.1 mole) of N-4-chlorobenzyl-N-cyclopentylamine were reacted with 13.5 grams (0.1 mole) of phenylisothiocyanate. 32 grams of N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea were obtained. Yield: 92%, Melting point: 129°-132° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04127673 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-c45d45730c5d4b50b13b1fe0493dcdd3 |
| Source note | uspto-grants-1978_11 |