HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diglyme → HCID 178420510, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diglyme | HCID 8150 | — |
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Reactant | 8-furfuryl-5-phenyloxy-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidine | HCID 22758530 | — |
| Product | HCID 178420510 | HCID 178420510 | — |
Reaction Steps
0.01 mol. of 8-furfuryl-5-phenyloxy-8H-pyrazolo-[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidine is heated in 50 ml. of diethyleneglycol dimethyl ether containing 0.01 mol. of selenium dioxide at reflux temperature with stirring for 2 hours. The mixture is filtered hot and evaporated to dryness. 5-Phenyloxy-8H-pyrazolo-[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidine remains.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04127655 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-3032e6dd8eef4e3d84440b490a58d8d2 |
| Source note | uspto-grants-1978_11 |