Aniline → N-phenyl-8-ethyl-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]-pyrimidin-5-amine

HRID 1704764Notes

Reaction equation

HRID 1704764 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.CN(C)CCCN.[C:15]([N:23]1[C:27]2[N:28]=[CH:29][C:30]3[C:31](OC4C=CC=CC=4)=[N:32][C:33]4[N:34]([N:36]=[CH:37][N:38]=4)[C:35]=3[C:26]=2[CH:25]=[N:24]1)(=O)[C:16]1C=CC=CC=1>>[C:2]1([NH:1][C:31]2[C:30]3[CH:29]=[N:28][C:27]4[N:23]([CH2:15][CH3:16])[N:24]=[CH:25][C:26]=4[C:35]=3[N:34]3[N:36]=[CH:37][N:38]=[C:33]3[N:32]=2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 3

HCID 6115AnilineHCID 7993N,N-Dimethyl-1,3-propanediamineHCID 227585058-Benzoyl-5-phenyloxy-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidine

Product 1

HCID 22758514N-phenyl-8-ethyl-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]-pyrimidin-5-amine

Procedure

By substituting aniline for the 3-dimethylaminopropyl amine in the procedure of Example 1 (c), N-phenyl-8-ethyl-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]-pyrimidin-5-amine is obtained.

Sources & evidence

ORD record
ord-07639115155a42d9bdcfaa754785a011
Source dataset
uspto-grants-1978_11
Patent number
US04127655

Reaction notes

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