HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Fluoride → HCID 22758933, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Fluoride | HCID 5235 | — |
| Reactant | Diglyme | HCID 8150 | — |
| Reactant | 3,3,4,4,5,5-Hexafluorooxolan-2-one | HCID 12561619 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22758933 | HCID 22758933 | — |
Reaction Steps
In accordance with the process of Example 1, sodium fluoride, diethyleneglycol dimethyl ether and perfluoro-γ-butyrolactone were charged in the autoclave, and the mixture of ethanol and diethyleneglycol dimethyl ether (2.5/1 by volume of the solvent/ethanol) was continuously fed with stirring at 6° to 10° C. until providing 1.1 molar ratio of ethanol perfluoro-γ-butyrolactone. The reaction was ceased at this ratio.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04127731 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-66372c3e29794491ad51d144b28c7353 |
| Source note | uspto-grants-1978_11 |