HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 54551503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | HCID 13734959 | HCID 13734959 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54551503 | HCID 54551503 | — |
Reaction Steps
The tartaric acid - mono - n - octylester is dissolved in tetrahydrofuran and treated with p-vinyl-anilinein presence of N,N'-dicyclohexyl-carbodiimide, D-Tartaric acid - mono - n - octylester (p-vinyl-anilide) is formed in high yields. This product is boiled with tri- (p-vinyl-phenyl)boroxine in benzene in a flask provided with a water separator. In nearly quantitative yield D-tartaric acid - mono - n - octylester - 2,3 -0- (p-vinyl-phenyl-boranate)- (p-vinylanilide) is formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04127730 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-55e3a074189e404ea8958159a97ae3d2 |
| Source note | uspto-grants-1978_11 |