HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanedithiol → N-[3-(3,4-dimethoxyphenyl)propyl]-N-methylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanedithiol | HCID 8013 | — |
| Reactant | N-Methylhomoveratrylamine | HCID 77039 | — |
| Reactant | 6-Chloro-1-(3,4-dimethoxyphenyl)hexan-1-one | HCID 22758344 | — |
| Reactant | HCID 54470276 | HCID 54470276 | — |
| Reactant | HCID 131711355 | HCID 131711355 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | N-[3-(3,4-dimethoxyphenyl)propyl]-N-methylamine | HCID 7131256 | — |
| Product | HCID 20509881 | HCID 20509881 | — |
Reaction Steps
6-chloro-3'4'-dimethoxyhexanophenone and N-methyl-homoveratrylamine. 2-(3,4-Dimethoxyphenyl)-N-[3,4-dimethoxyphenyl)-propyl]-N-methyl-m-dithiane-2-propylamine oxalate (1:1) of melting point 116°-118° C. (from acetone); starting from 1,3-propanedithiol and 3',4'-dimethoxy-4-[[(3,4-dimethoxyphenyl)-propyl]-methylamino]-butyrophenone, obtained from 3,4-dimethoxy-γ-chlorobutyrophenone and 3-(3,4-dimethoxyphenyl)-N-methylpropylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04127588 |
| Source dataset | uspto-grants-1978_11 |
| ORD ID | ord-e4cd4eae17284e96954a667cdd5b37f6 |
| Source note | uspto-grants-1978_11 |