HCID 22758384, compound → HCID 22758343, compound

HRID 1704803Notes

Reaction equation

HRID 1704803 reaction equation
Cl.[CH3:2][O:3][C:4]1[CH:5]=[C:6]([C:12]2([CH2:22][CH2:23][CH2:24][N:25]([CH3:35])[CH:26](C)[CH2:27]C3C=CC=CC=3)[S:17](=O)(=O)[CH2:16][CH2:15][CH2:14][S:13]2(=O)=O)[CH:7]=[CH:8][C:9]=1[O:10][CH3:11].[CH3:36][O:37][C:38]1[CH:39]=[C:40]([CH:65]=[CH:66][C:67]=1[O:68][CH3:69])[CH2:41]CN(C)CCCCC1(C2C=CC(OC)=CC=2OC)SCCCS1>CC(C)=O.C(OCC)(=O)C>[CH3:2][O:3][C:4]1[CH:5]=[C:6]([C:12]2([CH2:22][CH2:23][CH2:24][N:25]([CH2:26][CH2:27][CH2:41][C:40]3[CH:65]=[CH:66][C:67]([O:68][CH3:69])=[C:38]([O:37][CH3:36])[CH:39]=3)[CH3:35])[S:13][CH2:14][CH2:15][CH2:16][S:17]2)[CH:7]=[CH:8][C:9]=1[O:10][CH3:11]

Participants

4

Reactant 2

HCID 22758384HCID 22758384, compoundHCID 86736182HCID 86736182, compound

Product 1

HCID 22758343HCID 22758343, compound

Reagents, catalysts & solvents 1

HCID 21584569Ethylacetate acetoneSolvent

Procedure

2-(3,4-Dimethoxyphenyl)-N-methyl-N-(-methylphenethyl)-m-dithiane-2-propylamine-1,1,3,3-tetraoxide hydrochloride of melting point 185°-187° C. (from acetone/ethyl acetate), starting from 2-(3,4-dimethoxyphenyl)-N-methyl-N-(α-methylphenethyl)-m-dithiane-2-propylamine (prepared as described in Example 6).

Sources & evidence

ORD record
ord-e25e341bb091457e97bb53f0d7ad1a24
Source dataset
uspto-grants-1978_11
Patent number
US04127588

Reaction notes

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