HCID 54155772, compound → HCID 54432008, compound

HRID 1706010Notes

Reaction equation

HRID 1706010 reaction equation
[CH2:1]([CH:5]1[CH:13]2[C:9]([CH2:10][CH2:11][CH2:12]2)=[CH:8][C:7](=[O:14])[CH2:6]1)[CH:2]([CH3:4])[CH3:3]>[Pd]>[CH2:1]([CH:5]1[CH:13]2[CH:9]([CH2:10][CH2:11][CH2:12]2)[CH2:8][C:7](=[O:14])[CH2:6]1)[CH:2]([CH3:4])[CH3:3]

Participants

3

Reactant 1

HCID 54155772HCID 54155772, compound

Product 1

HCID 54432008HCID 54432008, compoundYield 95%

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

5-Isobutylbicyclo [4.3.0] non-1-en-3-one (25.4 g, 0.13 mol) is treated according to the procedure of Example 8 with 0.5 g of 5% palladium on carbon. Distillation gives 24 g (bp 90°-92° C. at 0.5 mm) of pure 5-isobutylbicyclo [4.3.0] nonan-3-one represented by the structure: ##STR11##

Workup

  1. distillationDistillation

Sources & evidence

ORD record
ord-17a7e998a9fa4136a93649857bafec50
Source dataset
uspto-grants-1980_06
Patent number
US04206089

Reaction notes

Loading…