beta-Naphthamidine → HCID 178513465, compound

HRID 1706085Notes

Reaction equation

[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:11]([NH2:13])=[NH:12].[N+:14]([C:17]1[CH:28]=[CH:27][C:20]([CH:21]=[CH:22][S:23](Cl)(=[O:25])=[O:24])=[CH:19][CH:18]=1)([O-:16])=[O:15]>>[N+:14]([C:17]1[CH:18]=[CH:19][C:20]([CH:21]=[CH:22][S:23]([NH:12][C:11]([C:2]2[CH:3]=[CH:4][C:5]3[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=3)[CH:1]=2)=[NH:13])(=[O:25])=[O:24])=[CH:27][CH:28]=1)([O-:16])=[O:15]

Participants

Reactant 2

HCID 193409beta-Naphthamidine

HCID 3480064-Nitrostyrylsulfonyl chloride

Product 1

HCID 178513465HCID 178513465, compound

Procedure

Reaction of β-naphthamidine with 4-nitrostyrylsulfonyl chloride according to the above procedure affords N-(4-NITROSTYRYLSULFONYL)-β-NAPHTHAMIDINE, m.p. 180°-182.5° C., by triturating with isopropanol.

Sources & evidence

ORD record: ord-168b5d334d0c43f28a4a47c1e5c66acd
Source dataset: uspto-grants-1980_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04206142

Reaction notes

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