Cyclopropylamine → HCID 178465747, compound

HRID 1706097Notes

Reaction equation

HRID 1706097 reaction equation
[CH:1]1([NH2:4])[CH2:3][CH2:2]1.[Cl:5][C:6]1[CH:21]=[CH:20][CH:19]=[C:18]([Cl:22])[C:7]=1[CH:8]=[CH:9][S:10]([N:13]=[C:14]([O-])[CH2:15]Cl)(=[O:12])=[O:11]>>[CH:1]1([NH:4][C:14](=[N:13][S:10]([CH:9]=[CH:8][C:7]2[C:18]([Cl:22])=[CH:19][CH:20]=[CH:21][C:6]=2[Cl:5])(=[O:12])=[O:11])[CH3:15])[CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 69828CyclopropylamineHCID 74054390N-(2,6-dichlorostyrylsulfonyl)chloroacetimidate

Product 1

HCID 178465747HCID 178465747, compound

Procedure

Reaction of Cyclopropylamine with N-(2,6-dichlorostyrylsulfonyl)chloroacetimidate according to the procedure of Example 32(b) affords N-cyclopropyl-N'-(2,6-dichlorostyrylsulfonyl) acetamidine, m.p. 121°-124° C. when crystallized from benzene.

Sources & evidence

ORD record
ord-cf013f2577e44a7e863e160ca6e26949
Source dataset
uspto-grants-1980_06
Patent number
US04206142

Reaction notes

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