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4-(Chloromethyl)-2-nitroanisole → N,N-dimethyl-N-(3-nitro-4-methoxybenzyl)-N-3-benzamidopropylammonium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Chloromethyl)-2-nitroanisole | HCID 80785 | — |
| 反応物 | N-(3-(dimethylamino)propyl)benzamide | HCID 2332594 | — |
| 生成物 | N,N-dimethyl-N-(3-nitro-4-methoxybenzyl)-N-3-benzamidopropylammonium chloride | HCID 86733005 | — |
反応手順
Proceeding in a manner similar to that described above in 1a, and using N-(3-dimethylaminopropyl)benzamide, and 3-nitro-4-methoxybenzyl chloride, there was obtained N,N-dimethyl-N-(3-nitro-4-methoxybenzyl)-N-3-benzamidopropylammonium chloride, as an off white solid which melted at 133°-136° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04206144 |
| 出典データセット | uspto-grants-1980_06 |
| ORD ID | ord-b2a05e6c3b3f4028823d908deebdaf8a |
| 出典メモ | uspto-grants-1980_06 |