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N-(3-(dimethylamino)propyl)formamide → N,N-dimethyl-N-(5-nitro-1-naphthylmethyl)-N-3-formamidopropylammonium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(3-(dimethylamino)propyl)formamide | HCID 80020 | — |
| 反応物 | 1-Chloromethyl-5-nitronaphthalene | HCID 226047 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | N,N-dimethyl-N-(5-nitro-1-naphthylmethyl)-N-3-formamidopropylammonium chloride | HCID 86733015 | — |
反応手順
Proceeding in a manner similar to that described above in B-8a, 29.9 parts of N-(3-dimethylaminopropyl)formamide and 44.3 parts of 5-nitro-1-chloromethylnaphthalene were interacted in 30 parts of water to obtain N,N-dimethyl-N-(5-nitro-1-naphthylmethyl)-N-3-formamidopropylammonium chloride. The product was not isolated but was used directly in solution for reduction of the nitro group.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04206144 |
| 出典データセット | uspto-grants-1980_06 |
| ORD ID | ord-46675f4e4ec642f88db6e000b9a4188c |
| 出典メモ | uspto-grants-1980_06 |