HuagongsheHuagongshe Chemistry Print Report · For research reference only
Homoveratrylamine → HCID 21406686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Homoveratrylamine | HCID 8421 | — |
| Reactant | 2-(2-Methylphenyl)oxirane | HCID 151042 | — |
| Solvent | Benzene | HCID 241 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 21406686 | HCID 21406686 | 36.2% |
Reaction Steps
Homoveratrylamine (13.6 g, 0.0753 mole) and o-methylstyrene oxide (10.1 g, 0.0753 mole) were stirred at 100° under argon for 16 hours and then diluted with benzene and hexane and cooled in ice. The solid which precipitated was filtered and recrystallized from benzene-hexane to give 8.6 g (36%) of 2-methyl-α-[N-(3,4-dimethoxyphenethyl)aminomethyl]benzyl alcohol, mp 91°-94°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04206210 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-5c415cad2e7840bb85063f0e28349eb6 |
| Source note | uspto-grants-1980_06 |