HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → 4-Benzyloxy-alpha-ethyldesoxybenzoin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 1-(4-Hydroxyphenyl)-2-phenylbutan-1-one | HCID 227278 | — |
| Catalyst | Potassium Iodide | HCID 4875 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-Benzyloxy-alpha-ethyldesoxybenzoin | HCID 18976513 | — |
Reaction Steps
A mixture of 4-hydroxy-α-ethyldesoxybenzoin (44.5 g.), sodium carbonate (18.5 g.), potassium iodide (1.4 g.) and benzyl chloride (19 ml.) in ethanol (350 ml.) and water (50 ml.) was stirred and heated under reflux for 8 hours. The mixture was cooled, filtered and the residue washed with water to give 4-benzyloxy-α-ethyldesoxybenzoin (54.3 g.), m.p. 71° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04206234 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-528364d8dd7c4792bab41a8275fa4036 |
| Source note | uspto-grants-1980_06 |