Ammonia → 3-Heptanamine

HRID 1706347Notes

Reaction equation

[CH3:1][CH2:2][CH:3](O)[CH2:4][CH2:5][CH2:6][CH3:7].[NH3:9]>>[CH3:1][CH2:2][CH:3]([NH:9][CH:3]([CH2:4][CH2:5][CH2:6][CH3:7])[CH2:2][CH3:1])[CH2:4][CH2:5][CH2:6][CH3:7].[CH3:1][CH2:2][CH:3]([NH2:9])[CH2:4][CH2:5][CH2:6][CH3:7]

Participants

Reactant 2

HCID 222Ammonia

HCID 115203-Heptanol

Product 2

HCID 342033-Heptanamine

HCID 20335303HCID 20335303, compound

Procedure

If heptan-3-ol is reacted similarly with ammonia at 130° C., 80% of theory of di-3-heptylamine, 18.5% of theory of 3-heptylamine and 0.5% of theory of unconverted alcohol are obtained.

Sources & evidence

ORD record: ord-c4baee552cfb450ebc56e58f31bad830
Source dataset: uspto-grants-1980_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04207263

Reaction notes

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