HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 20335783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 20520021 | HCID 20520021 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20335783 | HCID 20335783 | — |
Reaction Steps
60 grams of 2-benzoyl-3-nitro-6-chloropyridine were added in portions to a solution of 10 grams of sodium metal in 500 ml. of methanol at 50° C. with stirring, whereby the temperature gradually increased. Then the mixture was heated under reflux for four hours and subsequently treated with two liters of water. The precipitated crystals were filtered off with suction after one hour and recrystallized from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04207322 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-d40e677dbfbe4c6b9e91a0849298cbb6 |
| Source note | uspto-grants-1980_06 |