3-Hydroxy-3-methylglutaric acid monoamide, ammonium salt → 3-Hydroxy-3-methylglutaric acid monoamide

HRID 1706594Notes

Reaction equation

HRID 1706594 reaction equation
[NH4+].[OH:2][C:3]([CH3:12])([CH2:8][C:9]([O-:11])=[O:10])[CH2:4][C:5]([NH2:7])=[O:6]>O>[OH:2][C:3]([CH3:12])([CH2:8][C:9]([OH:11])=[O:10])[CH2:4][C:5]([NH2:7])=[O:6]

Participants

3

Reactant 1

HCID 1317117913-Hydroxy-3-methylglutaric acid monoamide, ammonium salt

Product 1

HCID 127207103-Hydroxy-3-methylglutaric acid monoamide

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of 1.78 g. (0.01 moles) of 3-hydroxy-3-methylglutaric acid monoamide, ammonium salt in 50 ml of water is passed through a 100 ml column of Dowex 50 (H+) resin. The resulting eluate is then evaporated to dryness to afford 3-hydroxy-3-methylglutaric acid monoamide.

Workup

  1. customThe resulting eluate is then evaporated to dryness

Sources & evidence

ORD record
ord-da5ee834c2df4373b59d3a098e62c848
Source dataset
uspto-grants-1980_06
Patent number
US04208204

Reaction notes

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