Ethanol → HCID 20334260, compound

HRID 1706718Notes

Reaction equation

HRID 1706718 reaction equation
C([O:8][C:9]1[C:18]([CH3:19])=[C:17]2[C:12]([CH:13]=[CH:14][C:15]([CH3:23])([CH2:20][CH2:21][CH3:22])[O:16]2)=[CH:11][CH:10]=1)C1C=CC=CC=1.[CH2:24](O)C>[C].[Pd]>[OH:8][C:9]1[C:18]([CH3:19])=[C:17]2[C:12]([CH:13]([CH3:24])[CH2:14][C:15]([CH2:20][CH2:21][CH3:22])([CH3:23])[O:16]2)=[CH:11][CH:10]=1

Participants

4

Reactant 2

HCID 702EthanolHCID 20334250HCID 20334250, compound

Product 1

HCID 20334260HCID 20334260, compoundYield 84.2%

Reagents, catalysts & solvents 1

HCID 178418390HCID 178418390, compoundCatalyst

Procedure

6.5 Grams of the compound obtained in (3) were subjected to catalytic reduction with 0.5 g. of 10% palladium-carbon and 50 ml of ethanol under atmospheric pressure. The subject compound in amount of 4.0 g. (yield: 84.2%) was thus obtained.

Workup

  1. custom(yield: 84.2%) was thus obtained

Sources & evidence

ORD record
ord-504af191a2d34f148b1d6b01b4abd322
Source dataset
uspto-grants-1980_06
Patent number
US04208426

Reaction notes

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