HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → HCID 19797975, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 2,3,5,6-Tetrachloroterephthaloyl chloride | HCID 12868 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19797975 | HCID 19797975 | — |
Reaction Steps
A mixture of 34 grams of tetrachloroterephthaloyl chloride in 85 ml. of tetrahydrofuran and 100 ml. of dioxane are charged to a 500 ml. flask. About 75 grams of ethylene glycol is added dropwise to the solution. This is followed by dropwise addition of 20 grams of pyridine over a period of one hour. The reaction mixture is stirred for 24 hours, and then the volume concentrated by distillation up to a temperature of about 120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04208502 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-86cac483f5f545a0a9bd48116f2935f1 |
| Source note | uspto-grants-1980_06 |