HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperonal → HCID 86737060, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperonal | HCID 8438 | — |
| Reactant | Benzyltriethylammonium hydroxide | HCID 74601 | — |
| Reactant | 3626-69-5 | HCID 5372413 | — |
| Product | HCID 86737060 | HCID 86737060 | — |
Reaction Steps
1 mol of piperonal is reacted with 1.1 mols of crotonic acid piperidide in the presence of 0.09 mol of triethylbenzylammonium hydroxide in 100 parts by volume of one of the solvents indicated in Table 3 which follows, under the conditions described in Example 1 to give piperonylidenecrotonic acid piperidide. The yields achieved are likewise indicated in Table 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04209445 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-15e7becdbe0e4ebcbe34eaf13385f276 |
| Source note | uspto-grants-1980_06 |