HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Chloromethyl)naphthalene → 3-(beta-Naphthyl)methyl-2-oxo-1-benzimidazolineacetic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Chloromethyl)naphthalene | HCID 75632 | — |
| Reactant | 2-Oxo-1-benzimidazolineacetic acid ethyl ester | HCID 20089203 | — |
| Product | 3-(beta-Naphthyl)methyl-2-oxo-1-benzimidazolineacetic acid ethyl ester | HCID 10247950 | 81% |
Reaction Steps
The procedure described in Example 1 was repeated (using the same molar proportions as before) except that 440 mg. (0.002 mole) of 2-oxo-1-benzimidazolineacetic acid ethyl ester and 353 mg. (0.002 mole) of 2-chloromethylnaphthalene were reacted to afford 583 mg. (81%) of 3-(β-naphthyl)methyl-2-oxo-1-benzimidazolineacetic acid ethyl ester, isolated as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04209527 |
| Source dataset | uspto-grants-1980_06 |
| ORD ID | ord-a280e0fc7436444d8d1a83b9220f6b67 |
| Source note | uspto-grants-1980_06 |