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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1707052Generated: October 30, 2026

Dimethylformamide dimethyl acetal → 3-Dimethylamino-3'-methoxyacrylophenone

https://huagongshe.com/reaction/1707052

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamide dimethyl acetalHCID 78373—
Reactant2-Propen-1-one, 1-(3-methoxyphenyl)-HCID 10261393—
Product3-Dimethylamino-3'-methoxyacrylophenoneHCID 42573796—

Reaction Steps

A mixture of 25 g. of m-methoxyacrylophenone and 25 ml. of dimethylformamide dimethylacetal is refluxed for 12 hours. Removal of any volatile material in vacuo gives a thick oil. Bulb to bulb distillation gives the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04209621
Source datasetuspto-grants-1980_06
ORD IDord-ea677c974b7646a59b9d2f032ec02da9
Source noteuspto-grants-1980_06