Ethyl orthoformate → HCID 15416706, compound

HRID 1707073Notes

Reaction equation

HRID 1707073 reaction equation
[NH:1]([C:3]1[N:8]=[C:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:6]=[CH:5][N:4]=1)[NH2:2].[CH:15](OCC)(OCC)OCC>>[C:9]1([C:7]2[CH:6]=[CH:5][N:4]3[CH:15]=[N:2][N:1]=[C:3]3[N:8]=2)[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 31214Ethyl orthoformateHCID 203333472-Hydrazinyl-4-phenylpyrimidine

Product 1

HCID 15416706HCID 15416706, compound

Procedure

A mixture of 2.0 g. of 2-hydrazino-4-phenylpyrimidine and 25 ml. of triethyl orthoformate is refluxed for 6 hours. On cooling the desired compound is removed by filtration, m.p. 232°-234° C. [This compound is cited J. Chem. Soc. Japan, Ind. Chem. Sect. 58, 440 (1955) as having m.p. 192° C. No description or preparation procedures are given.]

Workup

  1. additionA mixture of 2.0 g

Sources & evidence

ORD record
ord-b22d60c31cd149afa81f18af8e1b45db
Source dataset
uspto-grants-1980_06
Patent number
US04209621

Reaction notes

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