Triethyl orthoacetate → HCID 20333362, compound

HRID 1707075Notes

Reaction equation

HRID 1707075 reaction equation
[NH:1]([C:3]1[N:8]=[C:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:6]=[CH:5][N:4]=1)[NH2:2].[C:15](OCC)(OCC)(OCC)[CH3:16]>>[CH3:15][C:16]1[N:4]2[CH:5]=[CH:6][C:7]([C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=3)=[N:8][C:3]2=[N:1][N:2]=1

Participants

3

Reactant 2

HCID 66221Triethyl orthoacetateHCID 203333472-Hydrazinyl-4-phenylpyrimidine

Product 1

HCID 20333362HCID 20333362, compound

Procedure

A mixture of 2.0 g. of 2-hydrazino-4-phenylpyrimidine and 25 ml. of triethyl orthoacetate is refluxed for 8 hours. On cooling the desired compound is removed by filtration, m.p. 303°-306° C.

Workup

  1. additionA mixture of 2.0 g

Sources & evidence

ORD record
ord-ab312b9272f244a29f462a7f3d461e3a
Source dataset
uspto-grants-1980_06
Patent number
US04209621

Reaction notes

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