Ethyl orthopropionate → HCID 20333377, compound

HRID 1707077Notes

Reaction equation

HRID 1707077 reaction equation
[NH:1]([C:3]1[N:8]=[C:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:6]=[CH:5][N:4]=1)[NH2:2].[C:15](OCC)(OCC)(OCC)[CH2:16][CH3:17]>>[CH2:16]([C:17]1[N:4]2[CH:5]=[CH:6][C:7]([C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=3)=[N:8][C:3]2=[N:1][N:2]=1)[CH3:15]

Participants

3

Reactant 2

HCID 66995Ethyl orthopropionateHCID 203333472-Hydrazinyl-4-phenylpyrimidine

Product 1

HCID 20333377HCID 20333377, compound

Procedure

A mixture of 1.55 g. of 2-hydrazino-4-phenylpyrimidine and 25 ml. of triethyl orthopropionate is refluxed for 6 hours. On cooling the desired compound is obtained by filtration, m.p. 246°-247° C.

Workup

  1. additionA mixture of 1.55 g

Sources & evidence

ORD record
ord-545f027c415b48fe8af11af4e0aabdb0
Source dataset
uspto-grants-1980_06
Patent number
US04209621

Reaction notes

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