Benzylamine → HCID 178524828, compound

HRID 1707221Notes

Reaction equation

HRID 1707221 reaction equation
[CH2:1]([NH2:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH:9][C:10]1[CH:18]=[CH:17][CH:16]=[C:15]([OH:19])[C:11]=1[C:12]([OH:14])=[O:13]>CO>[OH:9][C:10]1[CH:18]=[CH:17][CH:16]=[C:15]([OH:19])[C:11]=1[C:12]([O-:14])=[O:13].[CH2:1]([NH3+:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 7504BenzylamineHCID 93382,6-Dihydroxybenzoic Acid

Product 1

HCID 178524828HCID 178524828, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Benzylamine (1.07 g; 10 mmol) was added dropwise to a solution of 2,6-dihydroxybenzoic acid (1.54 g; 10 mmol) in methanol (10 cm3). The mixture was left to stand at 20° C. overnight which resulted in the formation of pale pink crystals. The product was collected by filtration and recrystallized from water to produce white crystals. Found: C, 63.8%; H, 5.9%; N, 5.1%. Calculated for C14H15NO4 : C, 64.30%; H, 5.74%; N, 5.36%. M.pt. 182°-184° C.

Workup

  1. waitThe mixture was left
  2. customwhich resulted in the formation of pale pink crystals
  3. filtrationThe product was collected by filtration
  4. customrecrystallized from water
  5. customto produce white crystals

Sources & evidence

ORD record
ord-0ccdd9f3afb941fa8a4298879109d966
Source dataset
uspto-grants-1994_10
Patent number
US05352388

Reaction notes

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